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1.
《Advanced Powder Technology》2022,33(11):103833
Eliminating the gold preg-robbing effect of carbonaceous matter in carbonaceous gold ores is crucial for gold leaching. In this study, suspension oxidation roasting was proposed to accelerate the decarbonization of carbonaceous gold ore. The characteristics of oxidation reaction process and gas release were analyzed by TG-DTA-FTIR. The phase transformation and microstructure evolution of samples during roasting were analyzed by XRD, SEM and BET. The results show that the gold preg-robbing effect was eliminated after the gasification of carbonaceous matter, and the CaO generated by decomposition of carbonates can effectively capture the SO2. After roasting for 75 min at 650 °C in a 20% O2 atmosphere, the total carbon removal rate reached 99.42%, the distribution of exposed gold increased from 28.85% to 77.10% and the gold leaching efficiency increased from 4.55% to 84.83%. In addition, about 70% sulfur was mainly fixed in the roasted products in the form of sulfate. Therefore, the suspension oxidation roasting process is an efficient and clean pretreatment method for carbonaceous gold ores. 相似文献
2.
《International Journal of Hydrogen Energy》2022,47(67):29172-29183
To improve the safety of wet dust removal systems for processing magnesium-based alloys, a new method is proposed for preventing hydrogen generation. In this paper, hydrogen generation by Mg–Zn alloy dust was inhibited with six common metal corrosion inhibitors. The results showed that sodium dodecylbenzene sulfonate was the best hydrogen inhibitor, while CeCl3 enhanced hydrogen precipitation. The film-forming stability of sodium dodecylbenzene sulfonate was tested with different contents, temperatures, Cl? concentrations and perturbation rates. The results showed that this inhibitor formed stable protective films on the surfaces of Mg–Zn alloy particles, and adsorption followed the Langmuir adsorption model. 相似文献
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4.
The pressure drop prediction of wet gas across single-orifice plate in horizontal pipes had been solved satisfactorily under an annular-mist flow in the upstream of orifice plates. However, this pressure drop prediction is still not clearly determined when the upstream is in an intermittent flow or stratified flow, which is corresponding to a region of low FrG (gas phase Froude number) in the flow pattern map of wet gases. In this study, the wet gas pressure drop across a single-orifice plate was experimentally investigated in the low FrG region. By the experiment, the flow pattern transition in the downstream of single-orifice plates, as well as the effects of FrG and FrL (liquid phase Froude number) on ΦG (gas phase multiplier), were determined and compared when the upstream is in the flow pattern transition and the stratified flow region, respectively. Prediction performances were examined on the available pressure drop models. It was found that no model could be capable of jointly predicting the wet gas pressure drop in the low FrG region with an acceptable accuracy. With a new method of correlating FrG and FrL simultaneously, new correlations were proposed for the low FrG region. Among which the modified Chisholm model shows the best prediction accuracies, with the prediction deviations of ΦG being within 7% and 3% when the upstream is in flow pattern transition and stratified flow region, respectively. 相似文献
5.
Xiang-feng KONG Xing-xing JIANG Sheng-guo XUE Ling HUANG William HARTLEY Chuan WU Xiao-fei LI 《中国有色金属学会会刊》2018,28(3):534-541
Bauxite residue, a highly saline solid waste produced from digestion of bauxite for alumina production, is hazardous to the environment and restricts vegetation establishment in bauxite residue disposal areas. A novel water leaching process proposed here was used to investigate the dynamic migration and vertical distribution of saline ions in bauxite residue. The results show that water leaching significantly reduced the salinity of bauxite residue, leaching both saline cations Na+, K+, Ca2+ and anions CO2?3, SO2?4, HCO?3. Na+ and K+ migrated from 40–50 to 20–30 cm of the column, presenting a high migration capacity. The migration capacity of Ca2+ was lower and accumulated at 30–40 cm of the column. CO2?3 initially distributed at 20–30 cm of the column, subsequently transported to 30–40 cm of the column, and finally returned to 20–30 cm of the column along with evaporation. SO2?4 was originally distributed at 40–50 cm, but finally migrated to 20–30 cm of the column. Nevertheless, HCO?3 remained at the bottom of the column, and its migratory was less affected by evaporation. 相似文献
6.
The online measurement of wet gas with extremely-low liquid loading (Lockhart-Martinelli parameter lower than 0.02) remains a challenge. In this study, three types of throttle devices, Venturi, orifice plate and cone, are compared experimentally with air-water two-phase flow in a horizontal pipe of inner diameter of 50 mm. High-precision correlations are established to measure the gas and liquid flowrates via a single throttle device. Results show that the two-phase mass flow coefficient (K) of the three throttle devices all increase linearly with the liquid densiometric Froude number and the K correlations are established respectively to correct the gas mass flowrate deviation. The pressure loss ratio (δ) for Venturi is sensitive and monotonous to the liquid loading, which contributes to the high accuracy of liquid flowrate measurement. By incorporating the K correlations, both the gas and liquid mass flowrates can be predicted precisely. The relative error of the gas mass flowrate predicted by the Venturi is within ±2.0% at 95% confidence level, and that of the liquid mass flowrate is within ±15% at 90% confidence level. 相似文献
7.
针对湖南柿竹园铋精矿火法冶炼过程中存在的成本高、低浓度SO2和散烟排放污染环境、有价金属综合回收率低等问题, 以柿竹园铋精矿为原料, 提出了加压氧化氨浸分离铋与铜、硫的新工艺, 研究了氨水加入量、浸出温度、浸出时间、浸出压力及浸出液固比等因素对铜、硫、铋浸出率的影响。在氨水用量1.8 mL/g铋精矿、液固比4∶1、釜压2.8 MPa、浸出温度160 ℃、浸出时间5 h、搅拌速度600 r/min的优化工艺条件下, 铜、硫浸出率分别达93.57%和92.87%, 铋不浸出并以氧化铋形态全部入渣, 实现了铜、硫与铋的高效分离。 相似文献
8.
福建某斑岩型金矿品位低、规模大,金主要以自然金形式存在,可见金的粒度较粗,为高效利用该低品位金矿,开展新型浸金剂金蝉全泥浸出试验和柱浸试验,结果表明:全泥浸出在磨矿细度为-0.074 mm占80%、矿浆浓度25%、加石灰调pH 值11.0左右、初始金蝉浓度为500 mg/L和过程中控制金蝉浓度不小于300 mg/L条件下浸出20 h,金的浸出率为93.43%,金蝉耗量为1.02 kg/t;柱浸在矿石粒度为-30 mm条件下喷淋浸出23天,金累计浸出率和金蝉累计耗量分别为86.54%和1.22 kg/t。 相似文献
9.
10.
《能源学会志》2020,93(2):474-481
Removal of SO2 and NO emissions from coal-fired power plants have always been the focus in coal's utilization industries for which traditional wet desulfurization system hold the potential to achieve simultaneous removal of SO2/NOx. In this work, a novel liquid catalyst (tributyl phosphate, TBP) was investigated for the simultaneous removal of SO2 and NOx in a NO pre-oxidation (ozone oxidation) assisted process. The absorption process and reaction mechanism of SO2 and NO2 were studied in a small-scale experimental system, and the removal efficiency of pollutant and the key parameters were examined in a pilot-scale system. The results show that the removal efficiency of NO2 in traditional wet desulfurization system is only 20–40%; however greatly increases to >90% when TBP is added. Moreover, TBP can enhance the NO2 removal performance in the presence of SO2 due to the formation of TBP–NO2–SO32− complex. Considering the oily nature of TBP that can be easily separated, such addition strategy hold great potential for industrial SO2/NOx simultaneously removal. 相似文献